CHEM63002
Separation Science
20
Variable teaching patterns
Postgraduate Taught
Level 7
Department of Chemistry
1
FHEQ level (Framework for Higher Education Qualifications) ' Masters/Integrated Masters P4 '
European Credit Transfer & Accumulation System Rating : 10.0
<ul> <li> Principles and mechanisms of chromatographic separation</li> <li> Theoretical considerations of separation efficiency</li> <li> Instrumentation and methodology for analytical separation and detection (Gas Chromatography and Liquid Chromatography)</li> <li> Optimisation of separation through appropriate selection of equipment and methodology (Gas Chromatography and Liquid Chromatography)</li> <li> Research applications of Separation Science </li></ul><div> </div><div> </div>
<p>1. Introduce the fundamental operating principles of column chromatography.</p><p>2. Explain the instrumentation of separation and detection by gas chromatography and liquid chromatography.</p><p>3. Describe the methodology used to optimise chromatographic separations.</p><p>4. Highlight specific applications of these separation science techniques in the research literature. </p>
<div> </div><ul> <li> describe the fundamental principles and mechanisms of chromatography separations.</li> <li> describe the instrumentation commonly used in separation science</li> <li> explain the methodology of instrument optimisation based on the requirements of the analysis.</li> <li> compare and contrast examples of major commercially available chromatography systems </li></ul><div> </div>
<ul> <li> calculate the efficiency of separation given experimental parameters and predict performance changes under given conditions.</li> <li> perform calculations involving chromatographic parameters under given experimental conditions and interpret the results in terms of analytical performance.</li> <li> select and justify appropriate chromatographic conditions and detector technology to address given research problems.</li> <li> critically assess the choice of separation science methodology in selected examples from the research literature.</li></ul>
<ul> <li> perform modelling of the chromatographic process and method optimisation</li> <li> operate computer simulation packages to explain experimental data</li></ul>
<ul> <li> produce accurate, efficient and coherent reports on chromatographic separations and their analysis</li> <li> participate in online discussions and tutorial sessions using enhanced communication skills</li></ul>
<div> This unit is delivered entirely via distance learning, including assessment. The course runs over 10 weeks, with a nominal 15h/week of student work. </div><div> </div><div> A typical week consists of: - An overview of the material, presenting the learning objectives for the week. - Explanatory material (~5h of student activity/week) in the form of video lectures, the course text and links to further online resources. - Self-Study Exercises (~2h/week). These are formative, with feedback for them given in the tutorial. - Discussion (~1h/week). Students are encouraged to discuss the exercises and material in the forums where tutors will facilitate peer learning, providing feedback/input where necessary. - Formative Assessment (~1h/week). This is to highlight misconceptions ready for the tutorial. - Tutorial (~1h/week). Students will video conference with their tutor in groups of 6-8 to discuss and give/receive feedback. - Reflective journal (~1 h/week). Guided by questions related to weekly subject matter. </div><div> </div><div> There is also private study of ~4h/week consisting of: - Revision - Coursework e.g. critical analysis of research literature - Further practice (e.g. after the tutorials) - Independent/further study </div><div> </div><div> The times specified will vary greatly through the weeks. For example week 7 is mostly dedicated to performing the virtual lab experiment and producing a lab report. Week 10 will consist entirely of private study and summative assessment exercises. </div><div> </div><div> </div>
1
Written exam
25%
2
Written assignment (inc essay)
75%
CHEM63002 AS Online Conditions (Programme 09612)
N
<p>Quantitative Chemical Analysis (Ninth edition),Daniel C Harris & Charles A Lucy Macmillan Education (2015), Available as E-book through UoM, ISBN: 9781319154141 </p>
eAssessment
10
Lectures
10
Practical classes & workshops
1
Tutorials
3
0
176